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1 article(s) from Samanta, Dipak

Self-assembly of Ru₄ and Ru₈ assemblies by coordination using organometallic Ru(II)₂ precursors: Synthesis, characterization and properties

Sankarasekaran Shanmugaraju,
Dipak Samanta and
Partha Sarathi Mukherjee

Beilstein J. Org. Chem. 2012, 8, 313–322, doi:10.3762/bjoc.8.34

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Scheme 1: Possible octanuclear prism and tetranuclear macrocycle resulting from the combination of a tetraden...

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Scheme 2: Formation of the tetranuclear complexes (2a and 2b) upon the reaction of Ru(II)₂ based acceptors 1a...

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Figure 1: ¹H (left) and ¹⁹F (right) NMR spectra of tetranuclear macrocycle 2a recorded in CD₂Cl₂–CD₃OD with p...

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Figure 2: ESIMS spectrum of the macrocycle 2a recorded in acetonitrile. Inset: Experimentally observed isotop...

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Figure 3: A ball and stick representation of 2a with atom numbering. Color code: Ru = green; O = red; N = blu...

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Scheme 3: Formation of an octanuclear macrocycle 2c upon reaction of Ru(II)₂-based acceptors 1c with imidazol...

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Figure 4: ¹H (left) and ¹⁹F (right) NMR spectrum of the macrocycle 2c recorded in CD₃CN with the peak assignm...

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Figure 5: Side (left) and top (right) view of the energy-minimized structures of the octanuclear macrocycle 2c...

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Figure 6: UV–vis absorption spectrum (left) of macrocycles (2a–2c) recorded in CH₃CN at 298 K, and cyclic vol...

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Published 28 Feb 2012

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Self-assembly of Ru4 and Ru8 assemblies by coordination using organometallic Ru(II)2 precursors: Synthesis, characterization and properties

Self-assembly of Ru₄ and Ru₈ assemblies by coordination using organometallic Ru(II)₂ precursors: Synthesis, characterization and properties